E . Development and Evaluation of Methods

نویسندگان

  • Eugene R. Kennedy
  • Thomas J. Fischbach
  • Ruiguang Song
  • Peter M. Eller
  • Stanley A. Shulman
  • DeLon Hull
چکیده

1. Method Development . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36 a. Preliminary Experimentation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 b. Recovery of Analyte from Medium . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 c. Stability of the Analyte on the Medium . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38 2. Method Evaluation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 a. Feasibility of Analyte Generation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 b. Capacity of the Sampler and Sampling Rate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 c. Sampling and Analysis Evaluation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 d. Sample Stability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 e. Precision, Bias, and Accuracy . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43 3. Field Evaluation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44 4. Documentation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44 5. Appendix Accuracy and Its Evaluation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45 6. References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48 Figure 1. Nomogram Relating Accuracy to Precision and Bias . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50 Table I Values of the Bias and the Precision Required to . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51 Obtain Designated Accuracy in Percentage Units

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تاریخ انتشار 1999